Zirconocene catalyzed diastereoselective carbometalation of cyclobutenes† †Electronic supplementary information (ESI) available: Experimental procedures, spectroscopic data and copies of 1H and 13C NMR spectra. See DOI: 10.1039/c6sc02617f Click here for additional data file.
نویسندگان
چکیده
General Considerations: 1 Optimization of Reaction Conditions: 2 Experimental Section: 3 Procedure for the synthesis of (3-hexylcyclobut-2-en-1-yl)methanol (1b): 3 Procedure for the synthesis of (3-phenethylcyclobut-2-en-1-yl)methanol (1d): 3 General procedure for the synthesis of cyclobutene methylethers (1a/1c): 3 Typical procedure for the synthesis of 1-(((3-hexylcyclobut-2-en-1-yl)methoxy)methyl)4-methoxybenzene (1e): 4
منابع مشابه
Copper-catalyzed direct alkylation of heteroarenes† †Electronic supplementary information (ESI) available: Experimental procedures, characterization and copies of 1H and 13C NMR spectra for all new compounds. See DOI: 10.1039/c6sc05622a Click here for additional data file.
متن کامل
Enantioselective bifunctional iminophosphorane catalyzed sulfa-Michael addition of alkyl thiols to unactivated β-substituted-α,β-unsaturated esters† †Electronic supplementary information (ESI) available: Experimental procedures, spectroscopic data, copies of 1H and 13C NMR spectra and HPLC and GC chromatograms. See DOI: 10.1039/c6sc02878k Click here for additional data file.
متن کامل
Palladium-catalyzed ligand-promoted site-selective cyanomethylation of unactivated C(sp3)–H bonds with acetonitrile† †Electronic supplementary information (ESI) available: Experimental details including characterization data, copies of 1H, 13C NMR and NOESY spectra. See DOI: 10.1039/c5sc04066c Click here for additional data file.
Table of
متن کامل8-Styryl-substituted coralyne derivatives as DNA binding fluorescent probes† †Electronic supplementary information (ESI) available: Experimental procedures, additional spectroscopic data, 1H and 13C NMR spectra of 2 and 4a–f. See DOI: 10.1039/c6ra27684a Click here for additional data file.
متن کامل
Enantioselective synthesis of (–)-chloramphenicol via silver-catalysed asymmetric isocyanoacetate aldol reaction† †Electronic supplementary information (ESI) available: Experimental procedures, characterisation data, copies of 1H and 13C NMR spectra, and HPLC traces. See DOI: 10.1039/c5ob02141c Click here for additional data file.
متن کامل
ذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
عنوان ژورنال:
دوره 8 شماره
صفحات -
تاریخ انتشار 2017